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Yep, you can do that, or you can connect all three hard drives to the Sonnet controller for maximum performance (you may need to purchase an inexpensive UltraATA ribbon cable to do so, unless you've got another one).
That's the way I've got it hooked up in my computer -- Sonnet Tempo ATA/100 PCI card running three hard drives, two on one ribbon and one on the other.
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