| Linux & X don't do things the same - you might want to check out one of the BSD-based web sites for that kind of data.
Also realize that OS X does thigns a bit different than the others BSDs, so be careful.
A simpler way to do what you what is to boot into single-user mode (hold down Cmd+S at startup) and create symlinks to these other volumes for the folders you want:
i.e.
ln -s /Volumes/Disk2/Applications Applications
ln -s /Volumes/Disk3/Users Users
Just a suggestion.
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